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Disc1
| 1 | Heartbreaker (live, 1987) | Nirvana | 3:00 |
| 2 | Anorexorcist (radio performance, 1987) | Nirvana | 2:45 |
| 3 | Help Me I’m Hungry (radio performance, 1987) | Nirvana | 2:42 |
| 4 | White Lace and Strange (radio performance, 1987) | Nirvana | 2:09 |
| 5 | Mrs. Butterworth (rehearsal recording, 1988) | Nirvana | 4:05 |
| 6 | If You Must (demo, 1988) | Nirvana | 4:01 |
| 7 | Pen Cap Chew (demo, 1988) | Nirvana | 3:02 |
| 8 | Downer (live, 1988) | Nirvana | 1:43 |
| 9 | Floyd the Barber (live, 1988) | Nirvana | 2:33 |
| 10 | Raunchola / Moby Dick (live, 1988) | Nirvana | 6:25 |
| 11 | Beans (solo acoustic, undated) | Nirvana | 1:33 |
| 12 | Don’t Want It All (solo acoustic, undated) | Nirvana | 2:26 |
| 13 | Clean Up Before She Comes (solo acoustic, undated) | Nirvana | 3:13 |
| 14 | Polly (solo acoustic, 1988) | Nirvana | 2:30 |
| 15 | About a Girl (solo acoustic, 1988) | Nirvana | 2:45 |
| 16 | Blandest (demo, 1988) | Nirvana | 3:56 |
| 17 | Dive (demo, 1988) | Nirvana | 4:51 |
| 18 | They Hung Him on a Cross (demo, 1989) | Nirvana | 1:57 |
| 19 | Grey Goose (demo, 1989) | Nirvana | 4:36 |
| 20 | Ain’t It a Shame (demo, 1989) | Nirvana | 2:02 |
| 21 | Token Eastern Song (demo, 1989) | Nirvana | 3:21 |
| 22 | Even in His Youth (demo, 1989) | Nirvana | 3:13 |
| 23 | Polly (demo, 1989) | Nirvana | 2:37 |
Disc2
| 1 | Opinion (solo acoustic, 1990) | Nirvana | 1:34 |
| 2 | Been a Son (solo acoustic, 1990) | Nirvana | 1:13 |
| 3 | Lithium (solo acoustic, 1990) | Nirvana | 1:49 |
| 4 | Sliver (solo acoustic, 1989) | Nirvana | 2:10 |
| 5 | Where Did You Sleep Last Night? (solo acoustic, 1989) | Nirvana | 2:32 |
| 6 | Pay to Play (demo, 1990) | Nirvana | 3:29 |
| 7 | Here She Comes Now (demo, 1990) | Nirvana | 5:02 |
| 8 | Drain You (demo, 1990) | Nirvana | 2:38 |
| 9 | Aneurysm (demo, 1990) | Nirvana | 4:48 |
| 10 | Smells Like Teen Spirit (rehearsal demo, 1991) | Nirvana | 5:41 |
| 11 | Breed (Rough mix, 1991) | Nirvana | 3:08 |
| 12 | Verse Chorus Verse (outtake, 1991) | Nirvana | 3:18 |
| 13 | Old Age (outtake, 1991) | Nirvana | 4:20 |
| 14 | Endless, Nameless (radio appearance, 1991) | Nirvana | 8:48 |
| 15 | Dumb (radio appearance, 1991) | Nirvana | 2:35 |
| 16 | D‐7 (radio appearance, 1990) | Nirvana | 3:47 |
| 17 | Oh, the Guilt (B‐side, 1992) | Nirvana | 3:26 |
| 18 | Curmudgeon (B‐side, 1992) | Nirvana | 3:04 |
| 19 | Return of the Rat (Outtake, 1992) | Nirvana | 3:09 |
| 20 | Smells Like Teen Spirit (Butch Vig mix) | Nirvana | 4:59 |
Disc3
| 1 | Rape Me (solo acoustic, 1992) | Nirvana | 3:23 |
| 2 | Rape Me (demo, 1992) | Nirvana | 3:02 |
| 3 | Scentless Apprentice (rehearsal demo, 1992) | Nirvana | 9:33 |
| 4 | Heart‐Shaped Box (demo, 1993) | Nirvana | 5:32 |
| 5 | I Hate Myself and I Want to Die (B‐side, 1993) | Nirvana | 4:03 |
| 6 | Milk It (demo, 1993) | Nirvana | 4:35 |
| 7 | Moist Vagina (demo, 1993) | Nirvana | 1:57 |
| 8 | Gallons of Rubbing Alcohol Flow Through the Strip (B‐side, 1993) | Nirvana | 7:34 |
| 9 | The Other Improv (demo, 1993) | Nirvana | 6:24 |
| 10 | Serve the Servants (solo acoustic, 1993) | Nirvana | 1:36 |
| 11 | Very Ape (solo acoustic, 1993) | Nirvana | 1:53 |
| 12 | Pennyroyal Tea (solo acoustic, 1993) | Nirvana | 3:30 |
| 13 | Marigold (B‐side, 1993) | Nirvana | 2:34 |
| 14 | Sappy (B‐side, 1993) | Nirvana | 3:27 |
| 15 | Jesus Doesn’t Want Me for a Sunbeam (rehearsal demo, 1994) | Nirvana | 3:58 |
| 16 | Do Re Mi (solo acoustic, 1994) | Nirvana | 4:25 |
| 17 | You Know You’re Right (solo acoustic, 1994) | Nirvana | 2:31 |
| 18 | All Apologies (solo acoustic, undated) | Nirvana | 3:33 |